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Tantalum scrap of high oxygen content is recovered and processed to metallurgical grade tantalum by fine participation. Blending with carbon or other appropriate solid reducing agent, melting in a plasma furnace (20) at about tantalum melt temperature while suppressing partial pressure of tantalum oxide gas to minimize tantalum loss of the process.
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An experiment demonstrated the possibility of developing a zone refining process that would produce the first plutonium metal of extremely high purity. Plutonium rods containing known amounts of impurities were melted inside tantalum boats and passed horizontally through a threeturn, highfrequency ...
